Original document(5 pages)  中文版
    The disclosed synthesis method for Ir complex comprises: loading inert solvent with half volume of the three-necked flask, adding 1mmol IrCl3, and heating to full dissolution; dripping carefully 6-10mmol hexafluoroacetylacetone into the mixed liquid to react for 40-60h at 50-70Deg; filtering the white solid deposit to evaporate and dry; dissolving the obtained solid into 30ml inert solvent at 20Deg; filtering, putting the filtrate into icebox of 5Deg for 24h; finally, filtering, and vacuum drying. This invention solves the low-volatility problem of acetylacetone complex in prior art.
Application Number
申请号
200610041608 Application Date
申请日
2006.01.06
Title 名称 Iridium complex and its synthesis method
Publication Number
公开号
1803814 Publication Date
公开日
2006.07.19
Approval Pub. Date Granted Pub. Date
International Classification 分类号 C07F15/00
Applicant(s) Name
申请人
Northwestern Polytechnic University
Address 地址 710072
Inventor(s) Name 发明人 Zhang Qiuyu, Yan Xin, Zhang Hepeng
Attorney & Agent 代理人 huang yixin

  
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